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Place the open end of the tub closest to the thermometer bulb and 5-7 mm from its tip.
2. Immerse the tube and thermometer in hot oil bath that that has been prepared by your teacher. Be sure the entire capillary tub is immersed in the oil. Wait for your tube and thermometer to reach the temperature of the oil (approximately 100°C) Record the temperature of the bath.
3. After you tube and thermometer have reached constant temperature, lift them until only about one quarter of the capillary tube (open end down) is still in the oil bath. Pause for about 3 sec. to allow some oil to rise into the tube...
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