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The product was then distilled using a Hickman still and characterized using infrared spectroscopy. The percent yield of isopentyl acetate was 61.52%. This may have been low due to not all of the condensed product being removed from the Hickman still, some product being lost during transfer of the product from the reaction tube into the Hickman still, or the loss of some product due to evaporation during distillation. Infrared spectrum analysis of the product indicated that the product was isopentyl acetate, as expected, and thus that the reaction was successful.
Preparing Isopentyl Acetate by the Fischer Esterification
Introduction: The purpose of this experiment is to synthesize isopentyl acetate via an esterification reaction between acetic acid and isopentyl alcohol, using concentrated sulfuric acid as a catalyst...
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