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A strong exothermic reaction occurs. Once the reaction mixture is cooled in the fume cupboard (after about 10mins-15mins), the process of isolating the ester by solvent extraction and purifying it by distillation began.
The first step of purifying the ester was to add 100mL of water to the reaction mixture and transfer it to a 250mL separating funnel. A further 50mL of water was used to make sure all of the reaction mixture had been transferred to the separating funnel. The contents were swirled as well as making sure the pressure was vented using the venting procedure which was demonstrated, that is swirl the contents holding the lid with one hand and venting the gas pressure by using the other hand by opening the nozzle...
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