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Essay Details:
Essay text:
Concentrated phosphoric acid is corrosive. Mop up spillages immediately with plenty of water.
Cyclohexene and cyclohexanol are highly flammable. Keep away from naked flames. Anhydrous calcium chloride is an irritant.
PREPARATION
1) Weigh out between 9 and 10 grams of cyclohexanol directly into a 250cm3 round-bottomed, quickfit flask. Record accurately the mass of alcohol used.
2) Measure out 4cm3 of concentrated phosphoric acid in a small, glass measuring cylinder. Add this SLOWLY to the cyclohexanol in the flask and mix thoroughly by swirling cautiously.
3) Add an anti-bumping granule to the flask and set it up in the electric heating mantle with a reflux condenser fixed vertically to the top...
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