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The reaction would subsequently fail. Drierite was placed inside a plastic drying tube as a drying agent, absorbing all the moisture from the solvents that would later be refluxing in the apparatus and coming out into the atmosphere. After setting this up, researchers continued to crush magnesium turnings into smaller pieces in order to expose fresh metal by removing possible magnesium oxide that was on the surface of the turnings. The turnings were added to the round bottom flask as well as an iodine crystal, which facilitates the reaction by cleaning the surface of the magnesium metal. Bromobenzene and anhydrous diethyl ether were then added to the flask...
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