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The resulting mixture sat in an ice-water bath for 15 minutes. The solution was then allowed to sit for an additional 10 minutes to complete crystal formation. Recrystallization, TLC and melting point were used to identify and characterize the product of the reaction.
INTRODUCTION
The purpose of this experiment is to synthesize methyl nitrobenzoate from methyl benzoate, concentrated HNO3, and concentrated H2SO4 via an electrophilic aromatic substitution reaction. The product will then be isolated and recrystallized using methanol. Synthesis is an important tool for organic chemists. Many organic compounds containing aromatic rings are synthesized via electrophilic aromatic substitution...
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