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Chapter 28 Nitration Of Methyl Benzoate

Chapter 28: Nitration of Methyl Benzoate

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Title: Chapter 28: Nitration of Methyl Benzoate

Essay Details:

Subject: Science

Author: Tiffany H

Date: March 1, 2015

Level: University

Grade: B

Length: 2 / 465

Essay text:

This is a highly exothermic reaction and is kept under control by means of cooling; after which the mixture is poured onto ice. The solid product will then be isolated by filtration and recrystallized from methanol, in which it is very soluable. A.) Materials: 1) .6mL of concentrated sulfuric acid 2) .30g of methyl benzoate 3) Mixture of .2mL of concentrated sulfuric acid and .2 mL of concentrated nitric acid 4) Ice 5) .2 mL ice cold methanol B.) Procedure in Brief: 1) In a 10 x 100 mm reaction tube add .30g of methyl benzoate and .6 mL of concentrated sulfuric acid 2) Flick the tube or use magnetic stirring 3) Cool the mixture to 0 degrees Celsius 4) Add dropwise using a Pasteur pipette a mixture of ...

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