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Add .480mL of acetic anhydride and a drop of concentrated phosphoric acid. Drop in a magnetic spin vane and attach air condenser to vial. Partially submerge it in hot water. Stir with spin vane to dissolve salicylic acid. After mixture dissolves, heat for 8 to 10 minutes. Crystallize the Acetylsalicylic acid by cooling the mixture. Then add 3.0mL of water and stir.
Set up a Hirsh funnel for vacuum filtration. Add 1mL of cold water to help transfer all of crystallized substance. Rinse crystals with water once all collected in funnel. Let crystals dry in funnel. Let finish drying on a watch glass for the week...
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Common topics in this essay:
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- Acetylsalicylic Acid Synthesis
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- Separation Of A Carboxylic Acid, A Phenol, And A Neutral Substance
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