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The sample became a cloudy white color. The reaction vial was then connected to a reflux heating set-up and allowed to boil for twenty minutes until the cloudy white color dissolved into a clear liquid and then was allowed to cool. The sample was then transferred to a medium size beaker and slightly less than 2.5mL of sulfuric acid was added to the sample to adjust to pH 2. It was then placed in an ice bath to promote crystallization and then vacuum filtered to produce a white solid. The Salicylic Acid was the purified by adding 3mL of boiling water and then re-crystallization by placing it in an ice bath and vacuum filtering it...
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