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The first step of the experiment was the condensation of benzaldehyde to yield benzoin. Thiamine catalyst along with water and ethanol were added to the benzaldehyde, then NaOH was added until the solution turned yellow. After recrystallization, the product was benzoin. Step two was the oxidation of benzoin to benzil. Nitric acid was added to the benzoin and heated, this was followed by recrystallization to yield the benzil. In step three the benzil from step two was to be synthesized tetraphenylcyclopentadienone. The benzil and 1,3-diphenylacetone were mixed with ethanol. After heating this, ethanoic KOH was added and the solution was left to reflux...
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