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If the rotary evaporators are in use, leave them there.
e.When your dichloromethane has been removed, reweigh the flask to determine the mass of the unknown.
4.After you have isolated the unknown in step 3 above, scrape it out into a 125 mL Erlenmeyer flask. Any remaining unknown can be removed from the flask by rinsing the flask with a few mL of boiling water.
5.Be sure to allow your aspirin and unknown to dry thoroughly before you weigh them and determine their melting point ranges.
Lab Report Format for Separating the Components of "Panacetin" (2) and Recrystallization and Melting Point Measurement: Identifying the Components of "Panacetin" (3)...
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